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Load:
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1. komponenta
| Lecture type | Total |
| Lectures |
30 |
| Seminar |
15 |
* Load is given in academic hour (1 academic hour = 45 minutes)
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Description:
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COURSE CONTENT:
Electromagnetic radiation, molecule vibrations. Dispersive and Fourier transform infrared spectrometers. Transmission methods (near infrared, mid infrared and far infrared spectroscopy), internal and external reflectance methods (attenuated total reflectance, specular and diffuse reflectance), photoacoustic spectroscopy, infrared emission spectroscopy, infrared microscopy, coupled systems (chromatography - infrared spectroscopy, thermal analysis - infrared spectroscopy). Analysis and assignment of infrared spectra of organic and inorganic molecules. Biological, industrial and environmental applications.
Scattered radiation, polarized radiation. Dispersive and Fourier transform Raman spectrometers. Raman spectroscopy, resonance Raman scattering, surface-enhanced (resonance) Raman scattering, Raman microscopy, nonlinear Raman spectroscopy (hyper Raman spectroscopy, coherent anti-Stokes Raman scattering). Use of Raman spectroscopy in mineral, polymer and dye analysis, in art and archeology; biological, forensic and industrial applications.
LEARNING OUTCOMES:
To explain the interaction of electromagnetic radiation with matter in the IR and Raman spectroscopy.
To describe the techniques of IR spectroscopy based on the transmission, reflection and emission of radiation.
To describe the techniques of normal, resonance and surface-enhanced Raman spectroscopy.
To distinguish dispersive spectroscopy and Fourier transform spectroscopy.
To know the principle of imaging and mapping samples using vibrational microspectroscopy.
To describe the preparation of samples for qualitative and quantitative measurements, depending on the sample properties and the vibrational method.
To interpret infrared and Raman spectra.
To know the application of vibrational spectroscopy in the analysis of real samples, such as polymers, paints, paper, biological samples, drugs, food products, as well as various samples from the industry and the environment.
To select a suitable technique of vibrational spectroscopy for the analysis of an appropriate sample.
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Literature:
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- 1. B. Schrader (Ur.), Infrared and Raman Spectroscopy: Methods and Applications, Wiley-VCH, Weinheim, 1995.
2. Günzler, H.-U. Gremlich, Uvod u infracrvenu spektroskopiju, Školska knjiga, Zagreb, 2006.
3. E. Smith, G. Dent, Modern Raman Spectroscopy: A Practical Approach, John Wiley & Sons, Inc., Chichester, 2005.
- 1. B. Stuart, Infrared Spectroscopy: Fundamentals and Applications, John Wiley & Sons, Chichester, 2004.
2. R. Aroca, Surface-enhanced Vibrational Spectroscopy, John Wiley & Sons, Chichester, 2005.
3. J.M. Chalmers, P.R. Griffiths (ur.), Handbook of Vibrational Spectroscopy, John Wiley & Sons, 2001.
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Pristupačnost
