COURSE CONTENT:
Conductometry 1; conductivity measurements, examination of conductometry cells
Conductometry 2; conductance of strong and weak electrolytes, Kohlrausch law, conductivity measurements
Potentiometry 1; pH measurements, glass electrode
Potentiometry 2; potentiometric titration
Spectrophotometry; UV-Vis spectrophotometrs, Beer-Lambertov law
Transport number of ions; independent ion migration, Hittorf method
Calorimetry; calorimeters, determination of enthalpy of neutralization
Chemical kinetics; kinetics of decomposition of hydrogen peroxide.
LEARNING OUTCOMES:
EXPECTED COMPETENCES TO BE ACQUIRED:
After completing the laboratory course student should be able to:
- independently measure basic physico-chemical properties (pH, conductivity, absorbance, temperature, electromotive force, etc ...) using modern instrumentation and classical techniques
- collect and interpret the experimental results
- apply standard mathematical methods for solving the chemical problems and analysing the experimental results.
- apply various physico-chemical models for interpretation of experimental results
- analyse the experimental results regarding the reproducibility of measurements, sensitivity of measurements and predictable errors.
- analyse the factors that influence the obtained results.
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- N. Kallay, S. Žalac, D. Kovačević, T. Preočanin, i A. Čop, Osnovni praktikum fizikalne kemije, Fizikalno-kemijski praktikum I, skripta, drugo obnovljeno i dopunjeno izdanje, Fizičko-kemijski zavod, Kemijski odsjek, Prirodoslovno-matematički fakultet, Zagreb, 2002.
- T. Cvitaš, I. Planinić, N. Kallay: Rješavanje računskih zadataka u kemiji, II. dio, 2. izd., Hrvatsko kemijsko društvo, Zagreb, 2014., zbirka riješenih zadataka
- P. W. Atkins, J. De Paula: Elements of Physical Chemistry, 6. izd., Oxford University Press, Oxford 2013.
- T. Cvitaš: Fizikalna kemija, rukopis u pripremi
- P. W. Atkins, J. de Paula: Atkins' Physical Chemistry, 10. izd., Oxford University Press, Oxford, 2014.
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